Macroscale and Microscale Organic Experiments 7 ed. – Ebook PDF Instant Delivery – ISBN(s): 9780841238640,0841238642
Product details:
- ISBN-10 : 1305577191
- ISBN-13 : 978-1305577190
- Author: Kenneth L. Williamson, Katherine M. Masters
Succeed in your organic laboratory course with MACROSCALE AND MICROSCALE ORGANIC EXPERIMENTS, Seventh Edition. This proven, authoritative manual emphasizes safety and features new themed Modules experiments with real world applications. Using the manual’s mix of macroscale and microscale experiments, you’ll gain the knowledge and confidence you need to perform a wide variety of experiments, as well as experience working with conventionally-sized glassware.
Table contents:
1. Introduction.
2. Laboratory Safety, Courtesy, and Waste Disposal Techniques.
3. Melting Points and Boiling Points.
4. Recrystallization.
5. Distillation.
6. Steam Distillation, Vacuum Distillation, and Sublimation.
7. Extraction.
8. Thin-Layer Chromatography: Analysis of Analgesics and Isolating Lycopene from Tomato Paste.
9. Column Chromatography: Fluorenone, Cholesteryl Acetate, Acetylferrocene, and Plant Pigments.
10. Gas Chromatography: Analysis of Alkene Isomers.
11. Infrared Spectroscopy.
12. Nuclear Magnetic Resonance Spectroscopy.
13. Mass Spectroscopy.
14. Ultraviolet Spectroscopy, Refractive Indices, and Qualitative Instrumental Organic Analysis.
15. Computational Chemistry Elimination, Substitution, and Addition.
16. The SN2 Reaction: 1-Bromobutane.
17. Nucleophilic Substitution Reactions of Alkyl Halides.
18. Radical Initiated Chlorination of 1-Chlorobutane.
19. Alkenes from Alcohols: Cyclohexene from Cyclohexanol.
20. Bromination and Debromination: Purification of Cholesterol.
21. Dichlorocarbene Oxidation and Reduction.
22. Oxidation: Cyclohexanol to Cyclohexanone; Cyclohexanone to Adipic Acid.
23. The Cannizzaro Reaction: Simultaneous Synthesis of an Alcohol and an Acid in the Absence of Solvent.
24. Oxidative Coupling of Alkynes: 2,7-Dimethyl-3,5-octadiyn-2,7-diol.
25. Catalytic Hydrogenation.
26. Sodium Borohydride Reduction of 2-Methylcyclohexanone: A Problem in Conformational Analysis.
27. Epoxidation of Cholesterol.
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